Filtering apparatus



J. L. STEVENS Oct 11, 1932.

FILTERING APPARATUS Filed July 28, 1930 2 Sheets-Sheet V mv iwm N O 5 2m 2 m Oct. 11, 1932. J. L. STEVENS FILTERING APPARATUS I 2 Sheets-Sheet 2 Filed July 28, 1930 INVENTOR James L. 5fV/75' M w ATTORNEY Patented 05:. -11, 1932 UNITED STATES OFFICE JAMES L. STEVENS, OF HAYDEN, ARIZONA, ASSIGNOR TO RACONITE CHEMICAL COH- PANY, or HAYDEN, ARIZONA,

A CORPORATION OF ARIZONA.

surname APPARATUS Application filed July 28,

This invention relates to filtering devices and more particularly to rotary or continuous suction filters for separating solid particles from liquids, and has for its object certain provisions for improved method and apparatus for filtering. 0

One object of the present invention is to provide means for treating pulps containing course, heavy particles which are diflicult to handle in many types of apparatus now employed for filtering. Another object isto permit a classification of particles of different size so that the coarser particles may settle on the filter first. Another object is to provide efiicient means for removal of :the liquid drawn through the filter. Another object of the invention is to provide means for removing part of the liquid without filtering and also permit removal of the more dilute slime pulp without filtering so that the ma] or portion of this part of the liquid may be separated by settling and the thickened slime pul subsequently filtered. A further object is to provide an apparatus capable of conveying the filtered solids to a desired point of discharge, and to provide a convenient, simple means for effecting the discharge of such solids. Another object is to provide means for washing the semi-dehydrated solids between the point of feeding the apparatus and the point of discharging the filtered solids. Other objects of the present invention will be obvious in the following description.

In order to accomplish the above mentioned and other objects of the present invention, I have constructed a filtering apparatus com prising a plurality of filter compartments arrangedso as to form a shell of a frustum of a cone or polygonal pyramid having a porous filtering medium exposed at the inner surface and having a solid back or wall at the outer surface, with partitions and end walls so as to form compartments or recesses between the filtering medium and the solid back whereby suction and pressure may be applied separately to the filtering medium of the respective compartments at certain difi'erent positions during rotation.

The filter compartments are preferably equipped with a screen mounted between the amount of filtered solids.

1930. Serial No. 471,204.

filtering medium and the solid back so as to control the position of the filtering medium during the filtering operation and to provide ample space in the compartment for draining the filtered liquid.

The frustum of the cone or polygonal pyramid comprising the filtering compartments of the above described apparatus, preferably consists of a frustum of a cone or pyramid having approximately a 90 angle and truncated at a point approximately half-way between the apex and the periphery of the base. The frustum of the cone or erably placed in a semi-inverted position with the axis declining towards the apex end at an angle of approximately from the horizontal so that certain of the filter compartments assume a substantially horizontal'position, while opposite compartments assume a substantially vertical position. The position of the apparatus, may, however, be varied p somewhat. For example, the frustum of a 90 cone or pyramid comprising the filter compartments may be placed so that the axis declining towards the apex end forms, say, an angle of about 40 from the horizontal. The angle of the cone or polygonal pyramid comprising the filter compartments may also vary somewhat and may be greater or less than 90, but. should not be, however, sufiiciently acute or obtuse to hinder feeding and distributing the material to be treated, or to interfere in discharging the filtered solids from the apparatus. The size of the frustum, as related to a complete cone or pyramid, may also vary somewhat. However, the aperture at the truncated end should be sufficiently large to enable discharging the desired In the foregoing, I have designated a point approximately halfway between the apex and the periphery of the base as being the optimum point of truncation to form a sufficiently large aperture.

The frusto conical filter, shaped and disposed as above described, and having a plurality of segmental filtering elements disposed at diflerent angular positions about the axis thereof, is mounted in any suitable manner so as to permit rotation thereof about ts inclined axis, and suitable gears or other pyramid is pref- .10 the periphery means are provided for effecting such rotation.

A circular or annular battle is placed, preferably at right angles to the axis, at the truncated end of the filter apparatus, so as to restrict the aperture sufliciently to prevent unfiltered material flowing through said aperture and going with the filtered solids. Another circular or annular baflie is provided at of the base and preferably placed at right angles to the filtering medium so that a certain amount of unfiltered material may be retained in the apparatus. The outer bafile is provided with overflow aper' tures which prevent accumulating an excess of unfiltered material in the filtering apparatus, and also provides means for discharging liquid and/or pulp from the apparatus without filtering. i

In a preferred embodiment of the present invention, conduits are led from each of the various filter compartments along spoke-like members which extend from the filter towards the apex, to a valve device for applying 25 suction and pressure to the various filter compartments at certain different positions during rotation,

said valve device being located approximately at the apex end. The conduits are connected to the various filter compartments in such a manner as to provide eflicient draining of the filtered liquid.

The suction may be applied at any suitable point, but is preferably applied to each compartment when said compartment reaches approximately the position at which the filter medium thereof is brought into contact with the material to be filtered. I For example, the Suction may be applied at the lowest point during rotation or on the descending side somewhatin advance of this point, and may continue to a point in close proximity with the point of applying the pressure for dis charging the filtered solids.

The pressure is preferably applied at the point where the filter compartments approach the highest point and assume a vertical position. The pressure is effected by applying compressed air, steam, compartment. The compressed air passes through the filtering medium and assist in discharging the filtered solids therefrom.

The material to'be treated is preferably fed upon the filtering medium at or adjacent the point at which the suction is applied. The filtered solids are preferably discharged as V the filter compartments approach the highest point during rotation, and are caused to fall through the aperture at the truncated end of the apparatus and through apertures between the spoke-like members containing the conduits in communicating with the filter compartments and the valve device. A battle is provided to prevent the filtered product falling back into the unfiltered pulp.

In a preferred embodiment, the filter or the like to the filter,

apparatus is mounted on a frame with a pivot bearing at the apex end and with bearin wheels engaged in a circular track attached to the outer portion of the filter, so as to support the filter and permit the same to be rotated. The gear for driving or rotating the apparatus is conveniently placed in close proximity with the pivot hearing at the apex end. A housing is provided at the apex end to protect the gears, valve device, bearing, etc. from contact with the discharging filtered solids. It will be understood, however, that any suitable means may be employed for rotatably supporting said apparatus for rotation about its axis, and for driving the same.- In any case, however, such supporting and driving means should be so disposed as to permit free discharge of solids through truncated end of the filter, and suitable shield means may be provided, where necessary, to protect the parts from the discharged solids.

The apparatus is preferably provided with a scraper, preferably located at a point immediately following the blow or pressure, to assist in discharging the filtered solids. Another scraper is provided to prevent excess accumulation of filtered material on the spoke-like members.

From the foregoing description it is seen that the filtering apparatus of the present invention may be constructed to form the frustum of a cone or pyramid and therefore in some of the appended claims I have employed the term conoidal pyramid to include in 'a broad sense both a cone and a pyramid substantially as described. It will be observed that a cone may be considered as a special form of pyramld having an infinite number of sides, and that a polygonal pyramid approximates a cone more or less closely in any case. In either case, the respective segmental filtering compartments, and the filtering surfaces thereof, are inclined inwardly at an angle, say, between 40 and 50 toward the lower end of a common inclined axis of rotation, and the inclination of said filtering compartments and surfaces with respect to said axis of rotation is preferably approximately equal to the inclination of said axis with respect to the horizontal, so as to bring each filtering compartment approximately horizontal when in its lowermost or filtering position, the angle of the axis with respect to the horizontal varying somewhat, for example between 40 and 50i As stated above, however, the angle of the cone or pyramid comprising the filter compartments may be greater or less than 90 degrees, for example, the apex angle may vary between 80 and 100. In some cases, particularly with the larger apex angles, it may be advantageous to position the filter so that the angle of the axis with respect to the the central opening at the" horizontal is less than the angle of inclination of the surfaces of the filtering compartments with respect to the axis, in order that the surface of the filter compartments will more nearly approach the vertical when in their uppermost or discharging position, which is in general advantageous in promoting discharge of the solids by gravity through the central opening of the apparatus.

Referring to the accompanying drawings, formin part-of this specification and illustratingfiiy way of example one form of construction according to the present invention:

Fig. 1 is an inclined plan view, lookin into the base or open end of thefrustumshaped filter, with the outer baflie partly broken away.

Fig. 2 is a view principally in section on line 22 in Fig. 1, but with a portion of the -A lower part of the apparatus shown in elevation.

Fig. 3 is a sectional view of a filter compartment, and of the means for delivering material to be filtered, taken on line 33 in Fig. 1. i

Fig. 4 is a sectional view of one of the spoke-like frame members and the conduit aFssociated therewith, taken on line 44 in ig. 1. i

Fig. 5 is an enlarged face view of the retary valve plate.

Fig. 6 is an enlarged face view of the stationary valve plate.

Fig. 7 is a plan view of two adjacent filter compartments, showing a simple means of connecting the suction and pressure applying conduits thereto.

Fig. 8 is a section on line 8 -8 in Fig. 1, e means for washing the solids on the filter medium.

The filter is shown as comprising an annular series of filter compartments 1 disposed in the shape of a frustum of a polygonal or donoidal pyramid whose axis is positioned as above'stated, the individual filter compartments being disposed at different angular positions about said axis. The filter is provided with a battle member 2 at the inner or truncated end of the filter compartments defining a central aperture 50 through which the filtered solids may bedischarged, and with a battle member 3 at the outer rim of said filter compartments, said baflle members serving to maintain a supply of delivered material to be filtered upon the filtering medium of the filter compartments when in their lowermost or horizontal position. The outer bafiie 3 is provided with a plurality of angularly spaced overflow apertures 4 each communicating with a chute or trough 35 for discharging unfiltered liquid or slime pulp, it being understood that any suitable launder or other means may be provided for receiving the material so discharged.

The filter further comprises angularlyspaced spoke-like frame members 5 extending from the truncated end of the series of filter compartments toward the apex of the cone or pyramid and mechanically connected at their inner ends to a structure including bafile members 7 and 8 and rotary valve member 11.

valve plate 11 ismounted to rotate with the filter and is provided with a central projecting portion 11' secured to bearing sleeve 12, as by means of set screw 13. Said bearing g sleeve is rotatably mounted upon a stationary shaft 14 and engages against a shoulder 14 thereon, so that said shaft not only defines the axis of rotation of the filter, but also partially supports the weight thereof during rotation. bevel gear 15 is secured to the rotating valve member and provides a convenient means for rotating the filter. "A circular track 9 is secured outside the series of filter compartments and engages one or more bearing Wheels 10 to' assist in supporting the weight of the filter while rotating.

Referring particularly to F igs, 3 and 7 each filtercompartment is shown as provided with a filtering medium 23,- an intermediate screen 24 for controlling the position of the filtering medium during application of the suction, supporting members 25 for said screen, and a solid back or outer wall 26. Said members are secured together and supported at their sides and at the inner and outer ends in any suitable manner as, for ex-" ample, by frame members 27 secured together by bolts 27 and secured to the solid back or outer wall by bolts 28, said frame members serving also to enclose the sides and the inner and outer ends of the filter compartments. The frame members of adjacent compartments may also be secured together in any suitable manner, so as to form a complete rigidly connected filter. The central portion of the screen 24 for each compartment is preferably bowed or depressed outwardly away from the neutral position of the filtering medium, as shown, so that the filtering medium will be depressed upon application of suction and flattened toward the center of the filter upon application of pressure. A conduit is connected to the interior of each filter compartment, for example, by means of branch pipes or nipples 29 and 30 extending through the inner end wall thereof, the orifices in said nipples being preferably restricted so that the combined cross-sectional area thereof is not greater or bowed inwardly her and bears tightly eating with a, port or opening 22 extending throughthe lower face of said valve member.

The stationary valve member 16 surrounds the extension 11 of the rotating valve memagainst the lower face of said rotating valve member, and may be held in engagement therewith by any suitable means such as suitably mounted springs not shown. Said stationary valve member 18 provided with a suction compartment 17 and a pressure compartment 18 separated by partitions 19. The suction compartment 1s of relatively large angular extent and 1s connected to a vacuum line 17 for maintaining the desired suction therein and for withdrawing filtered liquid from the apparatus. The pressure compartment 18' is of relatively small angular extent and is connected to a pressure line 18 for supplying the desired ressure for loosening the filtered solids or filter cake from the filter medium. The suction compartment communicates with an opening or port 20 opening through the upper face of the stationary valve member in position to reigster successively with the ports or openings 22 in the rotating valve member from a position somewhat in advance of the lowermost position of the respective filter compartments to a position just slightly preceding the uppermost position thereof, while the pressure compartment communicates with an opening 21 also adapted to register with the successive openings22 when the respective filter compartments are substantially at their uppermost or vertical position. The direction of rotation of the apparatus is indicated by the arrows at A in Fig. 1 an Fig. 6. y I

The means for delivering the material to be filtered are shown as comprising launder 31 and spigot or pipe 32, which delivers the material upon a distributor box 33. Said distributor box extends inwardly over the filter compartments at a point somewhat in advance of the lowermost position thereof, and is open at the side from which the filter compartments approach the distributor, as shown at 33, so as to deliver the material to be filtered upon the filter medium of the respective filter compartments somewhat before they "reachtheir lowermost position. The distributor may advantageously be provided with a plurality of spaced baffle members 52 having inwardly inclined slots 53 therebetween so as to direct the feed inwardly of the filter compartments and cause uniform distribution of the material thereover. A stationary scraper 36 is provided in position to en gage the filter medium when the filter compartments pass their uppermost or vertical position and immediately following or concurrently with the application of pressure thereto, so as to assist in the discharging of filtered solids therefrom. A stationary battle 1 member 34 controls the direction of fall of the discharging solids and prevents stray portions of same from falling back into the unfiltered pulp. Scraper 36 and baffle 34 may be supported on a suitable supporting member 37 r- In the operation of the above described filtering aparatus, the filter is rotated about the axis of the conoidal pyramid at any desired rate of speed. Vacuum is applied through line 17 to the suction compartment of the valve and pressure through line 18 to the presure compartment. The material to be filtered, consisting for example of a suspension of both coarse particles and fine slimes in water or other liquid, is then delivered through launder 31 and distributor 33 upon the filtering medium of the filter compartments when in substantially their lowermost position or somewhat in advance thereof. The coarser particles settle first upon the filtering medium due to their greater weight, followed by a portion of the somewhat finer material, while the liquid to be filtered passes through the filter medium due to the suction within the filtering compartment and is removed through conduit 6 and vacuum line 17. In some cases, however, a considerable proportion of the finer slimes may remain in' suspension in the unfiltered material maintained upon the filtering medium, and the excess unfiltered material, containing these fine slimes but with the coarser particles substantially wholly removed therefrom, overflow through apertures 4 and discharge chutes 35.

In some operations it may be desirable d to wash the partially dehydrated solids prior to discharging same from the apparatus, and for such cases any suitable washing means may be provided. Spraying means 54, shown 5 in Figs. 1 and 8, provides a simple means for supplying water or other washing liquid to t the filtering medium during upward movement thereof and while still within the region of suction application.

As the filtering compartments rise upwardly, the material remaining thereon is filtered, and is also Washed if necessary, leaving a layer or cake of filtered solids on the surface of the filter medium. As each filterus ing compartment reaches a position adjacent the uppermost position thereof, the corne spondin the suction port 20 and comes into register with the pressure port 21. Pressure is thereno upon applied to the interior of said compartment, forcing the filtering medium outwardly away from the screen 24 into a substantially flat position or outwardly to a position bowed slightly away from the screen 125 member. The filtered solids are, therefore, loosened from the filtering medium not only by the outward pressure of the air or other pressure medium, but also due to'the bending or deformation port 22 passes out of register with of the filtering medium.

4 l5 tions.

The scraper 36 also assists in removal of the filtered solids from the filtering med um, and

the solids thus removed fall by gravity.

through the central aperture 50 onto any [6 suitable means for conveying the same away. The baflies 7 and 8 prevent these discharged solids from striking or collecting upon the valve mechanism, while the bafiie 34 prevents accidental return of such material to 10 the body of unfiltered material in the lower part of the filter. The filtering medium,

' having discharged the solids accumulated thereon, returns again to the lower part of the filter to undergo a new cycle of opera- 1 claim:

1. An apparatus for separating li uids from solids comprising a plurality of tering compartments disposed at different angular positions about a common axis and inclined inwardly toward a common apex at one end of said axis, each of said compartments having a thereof and a filteringmedium at the inside thereof,.means securing said filtering compartments together to form a filter, means supporting said filter in position with said common axis inclined downwardly toward said apex end thereof and in such manner as 80 to permit rotation of said filter about said axis, means for rotating said filter, means for applying suction to the respective filtering compartments when at the lower part of the filter and for applying pressure thereto when 85 at the upper part of the filter, and means for maintaining a supply of material to be filtered in contact with the filtering medium of the respective compartments when said compartments are in position for application of suction thereto, said filtering compartments terminating at their inner ends a suificient distance from said common apex to provide a F central opening therebetween for discharge of solids from the filtering medium. 2. An apparatus for separating solids from liquids comprising a filter formed as a frustum of a conoidal pyramid and having a lurality of filter compartments dispose at different positions about the axis thereof and rovided with filtering medium at the inner aces of said compartments, means rotatably supporting said filter with said axis inclined downwardly toward the apex end, means for rotating said filter about said axis, inwardly 55 projecting bafiles at the inner and outer edges of said filter defining a space inside the filter for receiving and maintaining material to be filtered upon the filtering medium of the respective compartments when in their lower- 0 most position, the baffle at the outer edge of the filter being provided with apertures permitting overflow of excess unfiltered material therethrough and the baifle at the inner edge thereof defining a central aperture for discharge of filtered solids therethrough,

solid wall at the outsidemeans for feeding material to be filtered to said material receiving space, means for applying suction to the respective filtering compartments and removing filtered liquids therefrom when in their lowermost position and during the upward movement thereof, and means for applying pressure to the respective filter compartments when adjacent their uppermost position.

An apparatus as set forth in claim 2,

and comprising in addition a scraper in osition to assist in dislodging filtered solids from the filtering medium when the compartments are adjacent their uppermost position.

4. A suction filtering apparatus for separating liquids from solids comprising a lurality of filtering compartments dispose at different angular positions about a common axis and inclined inwardly toward a common apex at one end of said axis, each of said compartments havin a solid wall atthe outside thereof and a filtering medium at the inside thereof, means securing said filtering compartments together to form a filter, means supporting said filter in position with said common axis inclined downwardly toward said apex end thereof and in such a manner as to permit rotation of said filter about said axis means for rotating sai filter, means for applying suction to the res ective filtering compartments when at the lower part of'the filter and for applying ressure thereto when at the upper part of t e filter, means for maintaining a supply of material to be filtered in contact with the filtering medium of the respective compartments when said compartments are in position for application of suction thereto, and baflle means at the inner and .outer edges of the filter ex tending inwardly toward said axis so as to retain material to be filtered thereon; the bafiie means at the outer edge having apertures permitting overflow of excess unfiltered material and said filtering compartments terminating at their inner ends a suificient distance from said common apex to provide a central opening therebetween for discharge of solids from the filtering medium. J

5. A suction filtering apparatus for separating liquids from solids comprising a plullli rality of filtering compartments disposedat difierent angular positions about a common axis and inclined inwardly at an angle of between 40 and 50 degrees toward a common apex at one end of said axis, each of said compartments havin a solid wall at the outside thereof and a lterin medium at the inside thereof, means securing said filtering compartments together to form a filter, means supporting said filter in position with said common axis inclined downwardly toward said apex end thereof at an angle with respect to the horizontal approximately equal to the inward inclination of the filtering compartments.with respect to said axis and in such" a manner as to permit rotation of said filter about said axis, means for rotating said filter, means for applying suction to the respective filtering compartments when at the lower part of the filter and for applying pressure thereto when at the upper part of the filter, and means for maintaining a supply of material to be filtered in contact with the filtering medium of the respective compartments when said compartments are in position for application of suction thereto, said filtering compartments terminating at their inner ends a sufficient distance from said commo'rfapex to provide a central opening therebetween for discharge of solids from the filtering medium.

6. A suction filtering apparatus for separating liquids from solids comprising a plurality of filtering compartments disposed at different angular positions about a common axis and inclined inwardly at an angle of approximately 45 toward a common apex at one end of said axis, each of said compartments having a solid wall at the outside thereof and a filtering medium at the inside thereof, means securing said filtering compartments together to form a filter, means supporting said filter in position with said common axis inclined downwardly toward said apex end thereof at an angle approximately equal to the inward inclination of the filtering compartments toward said axis and in such manner as to permit rotation of said filter about said axis, means for rotating' said filter, means for applying suction to the respective filtering compartments when at the lower part of, the filter and for applying pressure thereto when at the upper part of the filter, and means for maintaining a supply of material to be filtered in contact with the filtering medium of the respective compartments when said compartments are in position for application of suction thereto, said filtering compartments terminating at their inner ends a sufficient distance from said common apex to provide a central opening therebetween for discharge of solids from the filtering medium, means for controlling dischar e of filtered solids, and means for controlhng flow of unfiltered material.

7. apparatus for separating solids from liquids comprising a suction filter formed as a frustum of a conoidal pyramid and having a plurality of filter compartments disposed at different positions about the axis thereof and provided with filtering medium at the inner faces of said compartments, means rotatably supporting said filter with said axis inclined downwardly toward the apex end, means for rotating said filter about said axis, inwardly projecting bafiies at the inner and outer edges of said filter defining a space inside the filter for receiving and maintaining material to be filtered upon the filtering medium of the respective compartments when in their lowermost position,

at the inner ed e thereof defining a central aperture for therethrough.

8. An apparatus as set forth in claim 7, said apparatus also comprising a scraper in position to assist in dislodging filtered solids from the filtering medium when said compartments are adjacent their uppermost position.

9. An apparatus for separating liquids from solids comprising a suction filter formed as a frustum of a conoidal pyramid having an apex angle between 80 and 100 degrees and provided with filtering medium at the inner surface thereof, means defining a plurality of filtering compartments outside said filtering medium at different angular positions about the axis of the filter, means rotatably supporting said filter for rotation about said axis and with said axis inclined downwardly toward the apex end at an angle of between 40 and 50 degrees with respect to the hori: zontal, means for maintaining the supply of material to be filtered in contact with the filtering medium at the lower part of the filter, means for applying suction to the filterin com artments when at the lower part 0' the pressure to the filtering compartments when at the upper part of the filter, said filtering compartments terminating at their inner ends a sufficient distance from said common apex to provide a central opening therebetween for discharge ef solids from the filtering medium, bafile means at the inner edge of said filtering compartments to prevent overflow of unfiltered material at that point and to define said central opening, and means for discharging excess unfiltered material separately from said solids.

10. An apparatus for separating liquids from solids comprising a suction filter formed as a frustum of a conoidal pyramid having an angle of approximately 90 degrees and provided with filter medium at the inner surface thereof, means defining a plurality of enclosed filtering compartments outside said filtering medium at different angular positions about the axis of the filter, means rotatably supporting said filter about its axis and with said axis inclined downwardly toward the apex end at an angle of approximately 45 degrees with respect to the horizontal,

ischarge of filtered solids lter, and means for applyingmeans for rotating said filter, means for delivering and maintaining a supply of material to be filtered upon the filtering medium at the lower portion of the filter, means for applying suction to the respective filtering compartments and removing filtered liquid therefrom when at the lower part of the filter and during upward movement thereof, means for discharging the filtered solids from the respective filtering media when at the upper part of the filter, said filtering compartments terminating at their inner ends a sufficient distance from the common apex thereof to provide a central aperture therebetween for discharging filtered material, a baflle at the inner edge of said filtering compartments restricting the flow of unfiltered material and, defining said central aperture, and a baflie at the outer edge of the filter provided with apertures permltting overflow of excess unfiltered material therethrough. 11. An apparatus for separating solids from liquids comprising a suction filter formed as a frustum of a conoidal pyramid and having a plurality of filtering compartments disposed at different angular positions about the axis thereof, said compartments being provided with filtering medium at their inner faces, with solid walls at the outer faces thereof, and with means defining side and end walls so as to completely enclose the interior of each compartment, means rotatahly supporting said filter with said axis inclined downwardly toward the apex at an angle such that the filtering compartments extend approximately horizontally when in their lowermost position, means for rotating said filter about said axis, means for delivering and maintaining a supply of material to be 40 filtered upon the filtering medium of the respective compartments when adjacent their lowermost position, means for applying suction to the respective filtering compartments and removing filtered liquid therefrom when adjacent their lowermost position and during the upward movement thereof, said com partments terminating at their inner ends a sufficient distance from the common apex thereof to provide an aperture for discharging the filtered solids, means for discharging the filtered solids from the filtering medium of each compartment by gravity through said aperture when said compartment-is adjacent the uppermost position, and means for preventing discharge of the unfiltered material with the filtered solids.

In testimony whereof I have hereunto subscribed my name this 19th day of July, 1930.

JAMES L. STEVENS. 

